HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromocyclobutane → HCID 53784624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromocyclobutane | HCID 78110 | — |
| Reactant | HCID 178438014 | HCID 178438014 | — |
| Product | HCID 53784624 | HCID 53784624 | 32.4% |
Reaction Steps
This compound was prepared according to the method of Preparation 3, using 750 mg (3.67 mmol, 1.0 equiv) 3-ethyl-1H-indazole-6-carboxylic acid methyl ester and 0.38 mL (4.04 mmol, 1.1 equiv) cyclobutyl bromide as starting materials to give 307 mg (32%) of a clear oil: HRMS calcd for C15H18N2O2+H: 259.1447. Found: 259.14550.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262040B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-dce07301f5604737a3977754792974bb |
| Source note | uspto-grants-2001_07 |