HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromocyclohexene → HCID 54264252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromocyclohexene | HCID 137057 | — |
| Reactant | HCID 178438014 | HCID 178438014 | — |
| Product | HCID 54264252 | HCID 54264252 | 45% |
Reaction Steps
This compound was prepared according to the method of Preparation 1, using 750 mg (3.67 mmol, 1.0 equiv) 3-ethyl-1H-indazole-6-carboxylic acid methyl ester and 0.46 mL (4.04 mmol, 1.1 equiv) 3-bromocyclohexene as starting materials to give 467 mg (45%) of a clear oil: HRMS calcd for C27H20N2O2: 284.1525. Found: 284.1512.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262040B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-e684de9c4a8245b79245a3f1f50ff260 |
| Source note | uspto-grants-2001_07 |