O-Methylhydroxylamine hydrochloride → HCID 15545849, compound

Participants

Reaction Steps

This compound was prepared according to the method of Example 37, using 222 mg (0.704 mmol, 1.0 equiv)[(1-cyclopentyl-3-ethyl-1H-indazole-6-carbonyl)-amino]-acetic acid and 59 mg (0.704 mmol, 1.0 equiv) methoxylamine hydrochloride as starting materials to give 39 mg of a clear oil, which was crystallized from ether/hexanes to give 34 mg (14%) of white crystals: mp 135-136° C.; Anal. calcd for C18H24N4O3: C, 62.77; H, 7.02; N, 16.27. Found: C, 62.64; H, 6.87; N, 16.47.

Provenance & Evidence