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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1385117Generated: November 1, 2026

HCID 53875714, compound → HCID 86757151, compound

https://huagongshe.com/reaction/1385117

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53875714HCID 53875714—
CatalystPalladium hydroxideHCID 9942167—
ProductHCID 86757151HCID 8675715191.4%

Reaction Steps

This compound was prepared according to the method of Example 38, using 203 mg (0.467 mmol, 1.0 equiv) 1-cyclopentyl-3-ethyl-1H-indazole-6-carboxylic acid (2-benzyloxycarbamoyl-ethyl)-amide as starting material and 50 mg of Pd(OH)2/C (Pearlman's catalyst) as catalyst, to give 147 mg (91%) of a white powder: mp 166-169° C.; Anal. calcd for C18H24N4O3: C, 62.77;H, 7.02; N, 16.27. Found: C, 62.58; H, 7.12; N, 16.27.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06262040B1
Source datasetuspto-grants-2001_07
ORD IDord-2db094cb05df45b8a2580074eb7fdc6d
Source noteuspto-grants-2001_07