HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53875714, compound → HCID 86757151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53875714 | HCID 53875714 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | HCID 86757151 | HCID 86757151 | 91.4% |
Reaction Steps
This compound was prepared according to the method of Example 38, using 203 mg (0.467 mmol, 1.0 equiv) 1-cyclopentyl-3-ethyl-1H-indazole-6-carboxylic acid (2-benzyloxycarbamoyl-ethyl)-amide as starting material and 50 mg of Pd(OH)2/C (Pearlman's catalyst) as catalyst, to give 147 mg (91%) of a white powder: mp 166-169° C.; Anal. calcd for C18H24N4O3: C, 62.77;H, 7.02; N, 16.27. Found: C, 62.58; H, 7.12; N, 16.27.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262040B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-2db094cb05df45b8a2580074eb7fdc6d |
| Source note | uspto-grants-2001_07 |