HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86757152, compound → HCID 21360896, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86757152 | HCID 86757152 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Product | HCID 21360896 | HCID 21360896 | 78.1% |
Reaction Steps
This compound was prepared according to the method of Example 38, using 126 mg (0.290 mmol, 1.0 equiv) 1cyclopentyl-3ethyl-1H-indazole-6-carboxylic acid (benzyloxycarbamoyl-methyl)-methyl amide as starting material and 40 mg of Pd(OH)2/C (Pearlman's catalyst) as catalyst, to give 78 mg (78%) of a light tan powder: mp 63° C. (dec); HRMS calcd for C18H24N4O3+H: 345,19285. Found: 345.1912.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262040B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-5acc0b4ff84a4702bdd7c0fe19de5f1a |
| Source note | uspto-grants-2001_07 |