HuagongsheHuagongshe Chemistry Print Report · For research reference only
Adipic Acid → HCID 54052130, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Adipic Acid | HCID 196 | — |
| Reactant | Proline benzyl ester hydrochloride | HCID 2733413 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 54052130 | HCID 54052130 | 100.3% |
Reaction Steps
Using General Procedure A with 1.0 g (4.1 mmol) L-Proline benzyl ester hydrochloride and 300 mg (2.1 mmol) adipic acid afforded, after flash chromatography (EtOAc), 1.07 g (100%) of the title compound as a colorless oil. MS m/e (%): 521 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06262089B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-59f44fa4ced44e50b0135b1f99f62f85 |
| Source note | uspto-grants-2001_07 |