Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1385806Generated: November 2, 2026

7-Aminoheptanoic acid → HCID 86755329, compound

https://huagongshe.com/reaction/1385806

Reaction equation

Participants

RoleNameHCIDCharge
Reactant7-Aminoheptanoic acidHCID 13580—
ReactantDimethylacetamideHCID 31374—
ReactantHCID 21715954HCID 21715954—
ProductHCID 86755329HCID 86755329—

Reaction Conditions

Temperature80 °C

Reaction Steps

To a solution of 7-aminoheptanoic acid (0.8 g, 5.5 mmol) in DMA (20 mL) was added MDTA-Cl (X) (2.8 g, 4.2 mmol) and the mixture stirred at 80° C. for 24 h. DMA was removed. To the residue water was added. The solid material was collected and recrystallized from EtOH to furnish the pure title compound XIIIc (1.02 g, 31%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06264916B1
Source datasetuspto-grants-2001_07
ORD IDord-4ce8c8090fe34d86be0b4b77f7cc34e6
Source noteuspto-grants-2001_07