Lithium hydroxide, monohydrate → HCID 18518697, compound

HRID 1385966Notes

Reaction equation

HRID 1385966 reaction equation
C[O:2][C:3]([C:5]1([OH:17])[C:14]2[C:9](=[C:10]([O:15][CH3:16])[CH:11]=[CH:12][CH:13]=2)[CH2:8][CH2:7][CH2:6]1)=[O:4].O[Li].O>>[OH:17][C:5]1([C:3]([OH:4])=[O:2])[C:14]2[C:9](=[C:10]([O:15][CH3:16])[CH:11]=[CH:12][CH:13]=2)[CH2:8][CH2:7][CH2:6]1

Participants

3

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 70241958HCID 70241958, compound

Product 1

HCID 18518697HCID 18518697, compound

Procedure

Prepared according to the method described in Example 1(ii) above from 1-hydroxy-5-methoxytetralin-1-yl-carboxylic acid, methyl ester (1.11 g; 4.7 mmol; from step (i) above) and LiOH.H2O (0.395 g; 9.4 mmol). Yield 460 mg (36%).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-f10d5d7720a74ef1920a3675361ac96d
Source dataset
uspto-grants-2001_07
Patent number
US06265397B1

Reaction notes

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