Lithium hydroxide, monohydrate → 1626-04-6

HRID 1385969Notes

Reaction equation

HRID 1385969 reaction equation
[OH:1][C:2]1([C:12]([O:14]C)=[O:13])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH2:5][CH2:4][CH2:3]1.O[Li].O>>[OH:1][C:2]1([C:12]([OH:14])=[O:13])[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH2:5][CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 168937Lithium hydroxide, monohydrateHCID 11528561HCID 11528561, compound

Product 1

HCID 185186951626-04-6

Procedure

The sub-title compound was prepared according to the method described in Example 1(ii) above from 1-hydroxytetralin-1-yl-carboxylic acid, methyl ester (2.5 g; 12.1 mmol; from step (i) above) and LiOH.H2O (1.02 g; 24.2 mmol). Yield 400 mg (17%).

Sources & evidence

ORD record
ord-fddc07d412c34062bdaf03e021b25384
Source dataset
uspto-grants-2001_07
Patent number
US06265397B1

Reaction notes

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