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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 13867Generated: October 26, 2026

1,1,1,3,3,3-Hexafluoro-2-propanol → Tri-tert-butylphosphonium Tetraphenylborate

https://huagongshe.com/reaction/13867

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1,1,3,3,3-Hexafluoro-2-propanolHCID 13529—
ReactantTris(1,1-dimethylethyl)phosphineHCID 83681—
ReactantSodium TetraphenylborateHCID 2723787—
ProductTri-tert-butylphosphonium TetraphenylborateHCID 2313666377%

Reaction Steps

Tri-tert-butylphosphine is reacted with 1,1,1,3,3,3-hexafluoro-2-propanol and with sodium tetraphenylborate to produce tri-tert-butylphosphonium tetraphenylborate (77% yield). A similar process is described in which tricyclohexylphosphine is used as starting material to produce tricyclohexylphosphonium tetraphenylborate (77% yield) (see Nonpatent Document 7).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07728176B2
Source datasetuspto-grants-2010_06
ORD IDord-32062efb59614351b3cd53ae313ef854
Source noteuspto-grants-2010_06