1271-42-7 → Bis(eta-cyclopentadienyl) iron

HRID 1386963Notes

Reaction equation

HRID 1386963 reaction equation
[C-:1]1(C(O)=O)[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH-:9]1[CH:13]=[CH:12][CH:11]=[CH:10]1.[Fe+2:14]>CCC(C)=O>[CH-:1]1[CH:5]=[CH:4][CH:3]=[CH:2]1.[CH-:9]1[CH:13]=[CH:12][CH:11]=[CH:10]1.[Fe+2:14]

Participants

3

Reactant 1

HCID 157642301271-42-7

Product 1

HCID 7611Bis(eta-cyclopentadienyl) iron

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

Coating solutions were prepared by refluxing ferrocene carboxylic acid and Zr n-propoxide, at 1:1 and 1:2 molar ratios of Zr:Fc, in MEK. Films were then spin coated on TEC 15 and cured at 125° C. for 8 hours. The resulting coatings, up to 1 μm thick, were hard and stable in the electrolyte and colored at 1.3 V.

Workup

  1. customCoating solutions were prepared

Sources & evidence

ORD record
ord-f12aa174c81d417b93623ce94a24fa90
Source dataset
uspto-grants-2001_07
Patent number
US06266177B1

Reaction notes

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