HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10667130, compound → HCID 21182964, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10667130 | HCID 10667130 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 21182964 | HCID 21182964 | 93% |
Reaction Steps
By essentially following the procedure outlined in Example 1, Part D, the title compound was prepared from 2-(4-methoxyphenyl)benzo[b]thiophen-3-yl 4-methoxyphenyl ketone (Part B) as a yellow solid in 93% yield following radial chromatography (SiO2; gradient of 20-40% EtOAc in hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265575B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-4a06a6a8f502431cab6ef48a90c09a76 |
| Source note | uspto-grants-2001_07 |