HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10785526, compound → HCID 11791731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10785526 | HCID 10785526 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 11791731 | HCID 11791731 | 67% |
Reaction Steps
By essentially following the procedure detailed in Example 5, Part B, the title compound was prepared from methyl 4-[1-[2-(4-methoxyphenyl)benzo[b]thiophen-3-yl]ethenyl]phenyl ether (Part A) in 67% yield as a yellow solid following radial chromatography (SiO2; gradient of 20-40% EtOAc in hexanes).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265575B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-aa8d3c85fc3a4145ac63f249d4edce22 |
| Source note | uspto-grants-2001_07 |