HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18357191, compound → HCID 18357244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18357191 | HCID 18357191 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18357244 | HCID 18357244 | 71% |
Reaction Steps
By essentially following the procedure outlined in Example 1, part D, the title compound was prepared in 71% yield from 4-[2-(diethylamino)ethoxy]phenyl 2-(4-methoxyphenyl)benzo[b]thiophen-3-yl ketone (Part A) as an orange foam following flash chromatography (SiO2; 5% TEA in THF).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265575B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-41e6543e6d8343b692cf9f4126436b42 |
| Source note | uspto-grants-2001_07 |