HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 21182833, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Methyl 3-bromo-4-(bromomethyl)benzoate | HCID 10804694 | — |
| Product | HCID 21182833 | HCID 21182833 | 70% |
Reaction Steps
By following essentially the procedure of Example 137, Part B, the title compound was prepared from methyl 3-bromo-4-bromomethylbenzoate (Example 137, Part A) and dimethylamine (40%), in 70% yield. The flash chromatography was carried out by eluting with a gradient of hexanes(100-80%)/EtOAc(0-20%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265575B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-945f748f00d44130b1c7f98aec74c142 |
| Source note | uspto-grants-2001_07 |