HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 21182666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-Benzyloxy-2-dimethylaminobenzo[b]thiophene | HCID 10612994 | — |
| Reactant | HCID 21182684 | HCID 21182684 | — |
| Product | HCID 21182666 | HCID 21182666 | 70% |
Reaction Steps
The title compound was prepared in 70% yield by essentially following the procedures outlined in Example 39, Part B (except using thionyl chloride instead of oxalyl chloride) from 3-nitro-4-[(1-pyrrolidinyl)methyl]benzoic acid (Part C, above) and 6-benzyloxy-2-(dimethylamino)benzo[b]thiophene (Example 81, Part B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06265575B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-41964061540648ffbb9ee5c860693467 |
| Source note | uspto-grants-2001_07 |