HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54374393, compound → HCID 136016629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54374393 | HCID 54374393 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 136016629 | HCID 136016629 | — |
Reaction Steps
0.4 g 4-(2-propyl)-5-ethoxy-2-(2-benzyloxy-6-chlorophenyl)oxazole was dissolved in 10 ml ethyl acetate. To the solution, 5% palladium/carbon in an amount of 0.11 g was further added, and the solution was stirred under hydrogen atmosphere for 15-30 min. at room temperature. The solution reacted was filtrated, then the filtrate was condensed under reduced pressure, affording the objective substance in an amount of 0.28 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06268310B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-a71156645ffa4277a0459a22425fb0d8 |
| Source note | uspto-grants-2001_07 |