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HRID1387537

反应详情

EQUATION

反应方程式

HRID 1387537 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(C(=O)Nc2ccccc2)cc1N
HCID8426

3-Amino-4-methoxybenzanilide

C14H14N2O2

结构：O=[N+]([O-])c1cccc(N=C=S)c1
HCID19050

Benzene, 1-isothiocyanato-3-nitro-

C7H4N2O2S

PRODUCTS

生成物

1
结构：COc1ccc(C(=O)Nc2ccccc2)cc1NC(=S)Nc1cccc([N+](=O)[O-])c1
HCID10477320

未命名化合物

收率 87.6%

PROCEDURE

实验过程

Prepared according to the procedure described for Example 60 using 3-amino-4-methoxy-N-phenyl-benzamide (0.243 g, 1.0 mmol) and 3-nitrophenyl isothiocyanate (0.183 g, 1.0 mmol). Trituration in hexanes/ethyl acetate (4:1) gave the product (0.370 g); m.p. 188-189° C.

WORKUP

后处理

  1. customPrepared