HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Tolylisothiocyanate → HCID 54422588, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Tolylisothiocyanate | HCID 69304 | — |
| Reactant | 3-Amino-4-methoxy-N-(3,5-dimethylphenyl)-benzamide | HCID 16793959 | — |
| Product | HCID 54422588 | HCID 54422588 | 48.6% |
Reaction Steps
Prepared according to the procedure described for Example 102 using 3-amino-N-(3,5-dimethylphenyl)-4-methoxy-benzamide from Example 11 (0.542 g, 2.01 mmol) and 3-methylphenyl isothiocyanate (0.28 mL, 2.07 mmol) to afford the product (0.41 g); m.p. 188-189° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06268387B1 |
| Source dataset | uspto-grants-2001_07 |
| ORD ID | ord-1cc86f372ede4ec3bc0f521ed2e50f77 |
| Source note | uspto-grants-2001_07 |