Methanesulfonic Acid → HCID 20675238, compound

Participants

Reaction Steps

A one-liter four-necked round-bottom separable flask having a stirrer, a thermometer and a Dimroth reflux condenser was charged with 600 g of hexane and 114.18 g of monoallylamine, and 192.2 g of methanesulfonic acid was gradually dropwise added with cooling and stirring. A purified white precipitate was recovered by filtration and dried to quantitatively give a crystal of monoallylamine- methanesulfonate.

Provenance & Evidence