Methanesulfonic Acid → HCID 20675238, compound

HRID 1387609Notes

Reaction equation

HRID 1387609 reaction equation
[CH2:1]([NH2:4])[CH:2]=[CH2:3].[CH3:5][S:6]([OH:9])(=[O:8])=[O:7]>CCCCCC>[CH3:5][S:6]([OH:9])(=[O:8])=[O:7].[CH2:1]([NH2:4])[CH:2]=[CH2:3]

Participants

4

Reactant 2

HCID 6395Methanesulfonic AcidHCID 7853Allylamine

Product 1

HCID 20675238HCID 20675238, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

A one-liter four-necked round-bottom separable flask having a stirrer, a thermometer and a Dimroth reflux condenser was charged with 600 g of hexane and 114.18 g of monoallylamine, and 192.2 g of methanesulfonic acid was gradually dropwise added with cooling and stirring. A purified white precipitate was recovered by filtration and dried to quantitatively give a crystal of monoallylamine- methanesulfonate.

Workup

  1. temperaturea thermometer and a Dimroth reflux condenser
  2. additionwas gradually dropwise added
  3. temperaturewith cooling
  4. filtrationA purified white precipitate was recovered by filtration
  5. customdried

Sources & evidence

ORD record
ord-5272cbad51314cc68665b2f4905f06b5
Source dataset
uspto-grants-2001_07
Patent number
US06268452B1

Reaction notes

Loading…