反应详情

To a reaction vial with a TEFLON fluoropolymer magnetic stirring rod, 3 ml containing 0.2 M tert-butyl hydroperoxide and 0.2 M 3,5,5-trimethylhexanoic acid in isooctane was added. The reaction was started by addition of 200 mg of Candida antartica enzyme and about 10 mg of molsieves (3 grains). After twenty-fourand one-half hours, 11.2% conversion to tert-butyl peroxy-3,5,5-trimethylhexanoate was obtained as measured with GC.

1. additionwas added
2. additionThe reaction was started by addition of 200 mg of Candida antartica enzyme and about 10 mg of molsieves (3 grains)