HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 54435346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 53689540 | HCID 53689540 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54435346 | HCID 54435346 | — |
Reaction Steps
5.3 g of the title compound, in the form of an oil, which is purified by chromatography on silica gel (migrating agent: 9:1 petroleum ether/ethyl acetate), are obtained by the procedure described in Example (1a) from 11.2 g of 6-(2-cyclohexylethoxy)-2-methylenehexanoic acid ethyl ester and 13.7 g of m-chloroperbenzoic acid in 100 ml of methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04430339 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-40484e3933ae4caa8634a9057cc31751 |
| Source note | uspto-grants-1984_02 |