HRID1388139

反应详情

EQUATION

反应方程式

HRID 1388139 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1.18 g of the title compound, in the form of a yellowish oil, which is purified by chromatography on silica gel (migrating agent: 90:10 petroleum ether/ethyl acetate), are obtained by the procedure described in Example (1a) from 2.5 g of 8-cyclopropyl-2-methyleneoctanoic acid ethyl ester and 3.85 g of m-chloroperbenzoic acid in 30 ml of methylene chloride.

WORKUP

后处理

  1. custom1.18 g of the title compound, in the form of a yellowish oil, which is purified by chromatography on silica gel (migrating agent: 90:10 petroleum ether/ethyl acetate)
  2. customare obtained by the procedure