HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 53977619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 53902482 | HCID 53902482 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53977619 | HCID 53977619 | — |
Reaction Steps
2.2 g of the title compound, in the form of a colourless oil, which is purified by chromatography on silica gel (migrating agent: 90:10 petroleum ether/ethyl acetate), are obtained by the procedure described in Example (1a) from 5.42 g of 5-cyclooctyl-2-methylenevaleric acid ethyl ester and 5.55 g of m-chloroperbenzoic acid in 50 ml of methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04430339 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-054a474f45664e3186ec176535120c6c |
| Source note | uspto-grants-1984_02 |