m-Chloroperbenzoic acid → HCID 53815920, compound

Participants

Reaction Steps

2.2 g of the title compound, in the form of a colourless oil, which is purified by chromatography on silica gel (migrating agent: 90:10 petroleum ether/ethyl acetate; thin layer chromatography on silica gel with petroleum ether/ethyl acetate 9:1:Rf =0.5), are obtained by the procedure described in Example (1a) from 4.4 g of 5-cycloundecyl-2-methylenevaleric acid ethyl ester and 5.15 g of m-chloroperbenzoic acid in 40 ml of methylene chloride.

Provenance & Evidence