Sodium Hydroxide → HCID 86739208, compound

HRID 1388149Notes

Reaction equation

HRID 1388149 reaction equation
C([O:3][C:4]([C:6]1([CH2:9][CH2:10][CH2:11][CH:12]2[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]2)[CH2:8][O:7]1)=[O:5])C.[OH-].[Na+:19]>O1CCCC1>[CH:12]1([CH2:11][CH2:10][CH2:9][C:6]2([C:4]([O-:5])=[O:3])[CH2:8][O:7]2)[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17]1.[Na+:19]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 54018462HCID 54018462, compound

Product 1

HCID 86739208HCID 86739208, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

1.1 g of 2-(3-cyclohexylpropyl)-oxirane-2-carboxylic acid ethyl ester are stirred for 2 hours at room temperature with 4.58 ml of 1 N sodium hydroxide solution and 5 ml of tetrahydrofuran. The mixture is concentrated to half its volume and the crystals of the title compound which have been precipitated are filtered off. Mp 105°-110° C.

Workup

  1. concentrationThe mixture is concentrated to half its volume
  2. customthe crystals of the title compound which have been precipitated
  3. filtrationare filtered off

Sources & evidence

ORD record
ord-da9ac381eaa1468a86a31907693bb7b7
Source dataset
uspto-grants-1984_02
Patent number
US04430339

Reaction notes

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