HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 54295183, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 54183825 | HCID 54183825 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 54295183 | HCID 54295183 | — |
Reaction Steps
82.3 g of 4-(3-cyclohexylpropyloxy)-2-methylenebutyric acid ethyl ester, in the form of a colourless oil, which is purified by chromatography on silica gel (migrating agent: chloroform), are obtained by the procedure described in Example (1b) from 103.6 g of 2-(3-cyclohexylpropyloxy)-ethylmalonic acid ethyl ester, 11 g of paraformaldehyde, 105 ml of pyridine and 2.9 g of piperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04430339 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-dad19fc5f46b4d35a0182eb86525da29 |
| Source note | uspto-grants-1984_02 |