m-Chloroperbenzoic acid → HCID 53848094, compound

Participants

Reaction Steps

7.5 g of the title compound, in the form of a colourless oil, which is purified by chromatography on silica gel (migrating agent: 90:10 petroleum ether/ethyl acetate; thin layer chromatography on silica gel with petroleum ether/ethyl acetate 8:2: Rf =0.55), are obtained by the procedure described in Example (1a) from 13.1 g of 7-cycloheptyl-2-methyleneheptanoic acid ethyl ester and 12.0 g of m-chloroperbenzoic acid in 200 ml of methylene chloride.

Provenance & Evidence