HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-1-(3,4-dichlorophenyl)ethanone → HCID 13186365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-1-(3,4-dichlorophenyl)ethanone | HCID 244751 | — |
| Reactant | Sulfamoylthioacetamide | HCID 13186364 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13186365 | HCID 13186365 | — |
Reaction Steps
A mixture of sulfamoylthioacetamide (7.7 g., 0.05 mol) and 3,4-dichlorophenacyl bromide (13.4 g., 0.05 mol) in ethanol (50 ml) was heated at reflux for 2 hours. After cooling and filtration there was obtained 11.5 g. of the desired intermediate, m.p. 187°-190° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04431652 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-4bc93edf8b17496d9f2f00da02e1d16c |
| Source note | uspto-grants-1984_02 |