Alpha-Methylstyrene → HCID 20233174, compound

HRID 1388492Notes

Reaction equation

HRID 1388492 reaction equation
[CH2:1]=[CH:2][CH:3]=[CH2:4].[CH3:5][C:6]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[CH2:7]>O1CCCC1>[CH2:1]=[CH:2][CH:3]=[CH2:4].[CH3:7][C:6]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[CH2:5].[CH2:1]=[CH:2][C:3]1[CH:9]=[CH:8][CH:6]=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 7407Alpha-MethylstyreneHCID 78451,3-Butadiene2×

Product 1

HCID 20233174HCID 20233174, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The procedure of Example 7 was repeated with the exception that 0.95 milliliters of tetrahydrofuran was added prior to the butadiene polymerization and the α-methylstyrene was added at the end of the butadiene polymerization. The materials employed were as follows:

Workup

  1. additionwas added

Sources & evidence

ORD record
ord-b4ed5f7cd9434458b36fa08f17018b2c
Source dataset
uspto-grants-1984_02
Patent number
US04431777

Reaction notes

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