HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 20471303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | 1-[(2-Bromophenyl)methyl]-1H-imidazole | HCID 13269319 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20471303 | HCID 20471303 | — |
Reaction Steps
A solution of oxalic acid (0.14 g) in hot ethanol (10 ml) was added to a solution of 1-(2-bromobenzyl)imidazole (0.4 g) in hot ethanol (5 ml). After boiling for 10 minutes, the solution was evaporated under reduced pressure to afford a white solid. Recrystallisation of the solid from propan-2-ol gave 1-(2-bromobenzyl)imidazole hydrogen oxalate, m.p. 146°-147°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04431815 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-28788ca76f924c54b733c8a5c4f79006 |
| Source note | uspto-grants-1984_02 |