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HRID1388573

反应详情

EQUATION

反应方程式

HRID 1388573 的结构方程式

REACTANTS

反应物

3
结构：Oc1ccc(Cl)cc1Cl
HCID8449

2,4-Dichlorophenol

C6H4Cl2O

结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：COc1cc([N+](=O)[O-])c2nccc(C)c2c1Cl
HCID12049927

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc([N+](=O)[O-])c2nccc(C)c2c1Oc1ccc(Cl)cc1Cl
HCID13004202

5-(2,4-Dichlorophenoxy)-6-methoxy-4-methyl-8-nitroquinoline

C17H12Cl2N2O4

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCCO
溶剂HCID8076

2-Ethoxyethanol

C4H10O2

PROCEDURE

实验过程

The title compound was prepared from 5-chloro-6-methoxy-4-methyl-8-nitroquinoline from Example 1 (15 g, 0.06 mol), 2,4-dichlorophenol (38 g, 0.23 mol), potassium hydroxide (13.2 g, 0.24 mol) and 2-ethoxyethanol (150 mL) as described in Example 1. The yield was 14.5 g (64%), mp 165.5°-168°.