Ammonium Hydroxide → 3-Methylfuran-2-carboxamide

HRID 1388579Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1388579
[OH-].[NH4+:2].[CH3:3][C:4]1[CH:8]=[CH:7][O:6][C:5]=1[C:9](Cl)=[O:10]>>[CH3:3][C:4]1[CH:8]=[CH:7][O:6][C:5]=1[C:9]([NH2:2])=[O:10]

Komponenten

3

Edukt 2

HCID 14923Ammonium HydroxideHCID 27966743-Methylfuran-2-carbonyl chloride

Produkt 1

HCID 107253453-Methylfuran-2-carboxamide

Versuchsvorschrift

To a stirred flask containing excess concentrated ammonium hydroxide was added gradually 50 g of 3-methyl-2-furoyl chloride. The resulting mixture was extracted with dichloromethane. The extracts were dried, then evaporated to provide solid 3-methylfuran-2-carboxamide.

Aufarbeitung

  1. extractionThe resulting mixture was extracted with dichloromethane
  2. customThe extracts were dried
  3. customevaporated

Quellen und Nachweise

ORD-Eintrag
ord-f1ed42c968ef4aa0abeb6a8dfddffc7f
Quelldatensatz
uspto-grants-1984_02
Patentnummer
US04431831

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