HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131713396, compound → HCID 54132603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131713396 | HCID 131713396 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54132603 | HCID 54132603 | — |
Reaction Steps
A solution of the ester product from part (b) in methanol is treated with 10% palladium-carbon catalyst and hydrogenated in a Parr apparatus at an initial pressure of 45 psi. for 1.5 hours. The mixture is filtered through Celite and evaporated to dryness to give N-[N-[ethoxy(phenylmethyl)phosphinyl]-L-phenylalanyl]-L-leucine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04432972 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-568e055cade7457483ad66eeea2e32a2 |
| Source note | uspto-grants-1984_02 |