HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-1-(1-benzofuran-2-yl)ethan-1-ol → HCID 12816505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-1-(1-benzofuran-2-yl)ethan-1-ol | HCID 12814357 | — |
| Reactant | 1-(4-[3-Carbomethoxypropoxy]phenyl)propan-2-one | HCID 13079613 | — |
| Reactant | N-[2-(4-(3-carbomethoxyphenoxy)phenyl)-1-methylphenyl]-2-(2-benzofuranyl)-2-hydroxyethanamine | HCID 20470048 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12816505 | HCID 12816505 | — |
Reaction Steps
By a method analogous to that described in Example 2 but using 2-(2-benzofuranyl)-2-hydroxyethanamine (4.54 g) and 1-(4-[3-carbomethoxypropoxy]phenyl)propan-2-one (6.41 g), N-[2-(4-(3-carbomethoxyphenoxy)phenyl)-1-methylphenyl]-2-(2-benzofuranyl)-2-hydroxyethanamine was prepared, m.p. 63°-70° (Et2O) as a 37:63 mixture of diastereoisomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04432993 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-4ebfe79eed6743d9bbc828e9058979f1 |
| Source note | uspto-grants-1984_02 |