HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 70507384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15583504 | HCID 15583504 | — |
| Product | HCID 70507384 | HCID 70507384 | 92% |
Reaction Steps
11.5 g of 1-amidino-4-piperidineacetic acid prepared in Example 54 was dissolved in 100 ml of a 1 N hydrochloric acid solution, and the solution was treated with activated charcoal and concentrated. Acetone was added to the residue to obtain 12.7 g (yield: 92%) of 1-amidino-4-piperidineacetic acid hydrochloride as colorless prisms having a melting point of 213° to 215.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04433152 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-c8e669ab704740b087b53ced628a2ab7 |
| Source note | uspto-grants-1984_02 |