Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Chloride | HCID 6327 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 86739288 | HCID 86739288 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 86739289 | HCID 86739289 | — |
Reaction Steps
A 2-liter autoclave was charged with 858.3 gm. (2.4 mol) diethanol octadecyl amine, 20 gm. sodium bicarbonate and 420 ml. isopropyl alcohol. The temperature was raised to 100° C. Methyl chloride was introduced and was added periodically until the pressure remained constant (65 psig) for one hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04434076 |
|---|
| Source dataset | uspto-grants-1984_02 |
|---|
| ORD ID | ord-727cc7aa41e3415fbdd25201ee952eaa |
|---|
| Source note | uspto-grants-1984_02 |
|---|
