Methyl Chloride → HCID 86739289, compound

HRID 1388872Notes

Reaction equation

HRID 1388872 reaction equation
[CH2:1]([NH2:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[CH2:20]([OH:22])[CH3:21].[CH2:23]([OH:25])[CH3:24].C(=O)(O)[O-].[Na+].C[Cl:32]>C(O)(C)C>[Cl-:32].[CH3:20][NH2+:19][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[CH2:23]([OH:25])[CH3:24].[CH2:20]([OH:22])[CH3:21]

Participants

5

Reactant 3

HCID 6327Methyl ChlorideHCID 516892Sodium BicarbonateHCID 86739288HCID 86739288, compound

Product 1

HCID 86739289HCID 86739289, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Conditions

Temperature
100 °C

Procedure

A 2-liter autoclave was charged with 858.3 gm. (2.4 mol) diethanol octadecyl amine, 20 gm. sodium bicarbonate and 420 ml. isopropyl alcohol. The temperature was raised to 100° C. Methyl chloride was introduced and was added periodically until the pressure remained constant (65 psig) for one hour.

Workup

  1. additionA 2-liter autoclave was charged with 858.3 gm
  2. additionwas added periodically until the pressure
  3. customfor one hour

Sources & evidence

ORD record
ord-727cc7aa41e3415fbdd25201ee952eaa
Source dataset
uspto-grants-1984_02
Patent number
US04434076

Reaction notes

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