HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13132221, compound → HCID 12553985, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13132221 | HCID 13132221 | — |
| Catalyst | HCID 178418778 | HCID 178418778 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12553985 | HCID 12553985 | 89.5% |
Reaction Steps
14 g 4-hydrazino-6-methoxy-5-nitropyrimidine are dissolved in 3.6 liters of methanol and stirred for 10 hours at 40° C. with 61.9 g of freshly prepared silver (I) oxide. Then the mixture is filtered and the solution evaporated. 10.5 g 4-methoxy-5-nitropyrimidine with a melting point of 193° to 195° C. is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04434167 |
| Source dataset | uspto-grants-1984_02 |
| ORD ID | ord-a94305473fa0402984c79d8c5af02281 |
| Source note | uspto-grants-1984_02 |