HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54255784, compound → Ethyl 5-(3-chlorophenyl)isoxazole-4-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54255784 | HCID 54255784 | — |
| Reactant | Ethyl-2-benzoyl-3-dimethylaminopropenoate | HCID 54499154 | — |
| Product | Ethyl 5-(3-chlorophenyl)isoxazole-4-carboxylate | HCID 22221485 | 51% |
Reaction Steps
The procedure of Example 15 was employed utilizing ethyl-2-(3'-chlorobenzoyl)-3-dimethylaminopropenoate in lieu of ethyl-2-benzoyl-3-dimethylaminopropenoate to yield ethyl-5-(3'-chlorophenyl)-4-isoxazolecarboxylate (3.2 g.; 51% yield) having a melting point of 75°-77° C. and the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04243406 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-2f23c084072246279a3b9f9994bdf5be |
| Source note | uspto-grants-1981_01 |