HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → HCID 20298518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | Octylamine | HCID 8143 | — |
| Reactant | o-(Methylthio)phenol | HCID 61261 | — |
| Product | HCID 20298518 | HCID 20298518 | 18% |
Reaction Steps
Reaction of the epichlorhydrin derivative of 2-(methylthio)phenol (14 g., 0.071 mole) with n-octylamine (9.04 g., 0.07 mole) according to the procedure of Example 2(b) and crystallization of the crude product from methanol-ether affords an 18% yield of analytically pure 1-[2-(methylthio)phenoxy]-3-(octylamino)-2-propanol hydrochloride, m.p. 105.5°-107.5° (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04243681 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-604b307602064f39ad8000ef7f16102c |
| Source note | uspto-grants-1981_01 |