HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichlorobenzoyl chloride → HCID 20298487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichlorobenzoyl chloride | HCID 66645 | — |
| Reactant | 2-Butanamine, 2-methyl- | HCID 68986 | — |
| Reactant | Ethyl 4-bromobutyrate | HCID 76300 | — |
| Product | HCID 20298487 | HCID 20298487 | — |
Reaction Steps
Analogously to Example 1, ethyl N-(2,4-dichloro)-benzoyl-4-[(1,1-dimethylpropyl)amino]butyrate (M.P. 75° to 77°) is obtained by reacting the reaction product of ethyl 4-bromobutyrate and 1,1-dimethylpropylamine with 2,4-dichlorobenzoyl chloride, the saponification of which yields 2,4-dichlorobenzoyl-4-[(1,1-dimethylpropyl)amino]-butyric acid (M.P. 124° to 126°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04243678 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-faed4a1edccf4ea29b44add72d8c4808 |
| Source note | uspto-grants-1981_01 |