HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoisovaleric acid → HCID 54166781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoisovaleric acid | HCID 11268 | — |
| Reactant | 1,3-Benzodioxol-5-amine | HCID 84310 | — |
| Product | HCID 54166781 | HCID 54166781 | — |
Reaction Steps
Following the procedure of Example 1, the m-phenoxybenzyl ester of α-bromoisovaleric acid is reacted with 3,4-methylenedioxyaniline (3equivalents) at about 75° for about 14 hours to yield the m-phenoxybenzyl ester of N-(3,4-methylenedioxyphenyl)valine, MS m/e 419 (M+, 13.2), 192 (100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04243819 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-d5bd3d94e17945b49e210896e359d031 |
| Source note | uspto-grants-1981_01 |