HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 53827115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | Tetrahydrofuran ethanol | HCID 21873804 | — |
| Reactant | HCID 136335629 | HCID 136335629 | — |
| Product | HCID 53827115 | HCID 53827115 | — |
Reaction Steps
Reaction of 7-chloro-5-(2-fluorophenyl)-N-hydroxy-α-nitro-3H-1,4-benzodiazepine-2-methanimine with pyrrolidine in tetrahydrofuran overnight at room temperature yielded yellowish crystals. For analysis a sample was recyrstallized from tetrahydrofuran/ethanol, mp 175°-178° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04244868 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-8d96408e37434a078099d68ee726209d |
| Source note | uspto-grants-1981_01 |