Tert-Butylamine → HCID 20296725, compound
Reaction equation
[C:1]([NH:5][C:6](=[O:20])[NH:7][C:8]1[CH:13]=[CH:12][C:11]([C:14](=[O:17])[CH2:15]Br)=[CH:10][C:9]=1[C:18]#[N:19])([CH3:4])([CH3:3])[CH3:2].O(C(NC1C=CC(C(=O)CBr)=CC=1C#N)=O)C1C=CC=CC=1.[C:43]([NH2:47])([CH3:46])([CH3:45])[CH3:44]>>[C:18]([C:9]1[CH:10]=[C:11]([CH:14]([OH:17])[CH2:15][NH:47][C:43]([CH3:46])([CH3:45])[CH3:44])[CH:12]=[CH:13][C:8]=1[NH:7][C:6]([NH:5][C:1]([CH3:4])([CH3:3])[CH3:2])=[O:20])#[N:19]Participants
4
Procedure
The 4'-(3-tert.butylureido)-2-bromo-3'-cyano-acetophenone used as starting material was prepared by reaction of 4'-phenoxycarbonylamino-2-bromo-3'-cyano-acetophenone and tert.butylamine at room temperature.
Sources & evidence
- ORD record
- ord-89847012afb74a59835e664945a29275
- Source dataset
- uspto-grants-1981_01
- Patent number
- US04244967
Reaction notes
Loading…