HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1389550Generated: October 31, 2026
Carbon Disulfide → 1-(2-Hydroxyethyl)-4-phenylimidazolidine-2-thione
https://huagongshe.com/reaction/1389550
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | HCID 13035411 | HCID 13035411 | — |
| Solvent | 1,1,1,2-Tetrachloroethane | HCID 12418 | — |
| Product | 1-(2-Hydroxyethyl)-4-phenylimidazolidine-2-thione | HCID 20485995 | — |
Reaction Steps
The methoxyethylamine product of Example IV in the amount of 4.5 g is dissolved in 20 ml of tetrachloroethane, and is stirred with 2 ml carbon disulfide at room temperature for one hour. The resulting slurry is then slowly heated to 120° C. and maintained at that temperature for four hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04245102 |
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| Source dataset | uspto-grants-1981_01 |
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| ORD ID | ord-77229deeb7754368a97c1003b413c1f5 |
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| Source note | uspto-grants-1981_01 |
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