HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178526276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178419752 | HCID 178419752 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178526276 | HCID 178526276 | — |
Reaction Steps
0.6 g. of 2-[(2,6-dichlorophenyl)imino]-1-hydroxyimidazolidine hydrobromide is dissolved in a little water and the pH is adjusted to 10 with 1 N caustic soda solution. The precipitate formed is extracted with methylene chloride. The organic extracts are dried over sodium sulfate and evaporated to dryness. The residue is recrystallized from acetonitrile, whereupon 2-[(2,6-dichlorophenyl)imino]-1-hydroxyimidazolidine, m.p. 215° (decomp.) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04244957 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-6620221c134448888c811bd3bfdbcad2 |
| Source note | uspto-grants-1981_01 |