Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1389617Generated: October 31, 2026

Ethanol → HCID 20297261, compound

https://huagongshe.com/reaction/1389617

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantChloroformHCID 6212—
ReactantThiophenolHCID 7969—
ReactantPotassium HydroxideHCID 14797—
Reactant3-PhenoxybenzaldehydeHCID 38284—
ProductHCID 20297261HCID 2029726165%

Reaction Steps

1.10 g of 3-phenoxybenzaldehyde, 1.65 g of thiophenol and 1.8 g of chloroform were dissolved in 5 ml of ethanol, and to the resulting solution was added dropwise a solution of 2.0 g of potassium hydroxide in 10 ml of ethanol over a period of 90 minutes. The reaction mixture was then stirred overnight at room temperature and then worked up in the same manner as described in Example 1 to obtain 1.10 g (65% yield) of 2-phenylthio-2-(3-phenoxyphenyl)acetic acid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04245108
Source datasetuspto-grants-1981_01
ORD IDord-94cc084482774713b81d526f633a1324
Source noteuspto-grants-1981_01