HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20297261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 3-Phenoxybenzaldehyde | HCID 38284 | — |
| Product | HCID 20297261 | HCID 20297261 | 65% |
Reaction Steps
1.10 g of 3-phenoxybenzaldehyde, 1.65 g of thiophenol and 1.8 g of chloroform were dissolved in 5 ml of ethanol, and to the resulting solution was added dropwise a solution of 2.0 g of potassium hydroxide in 10 ml of ethanol over a period of 90 minutes. The reaction mixture was then stirred overnight at room temperature and then worked up in the same manner as described in Example 1 to obtain 1.10 g (65% yield) of 2-phenylthio-2-(3-phenoxyphenyl)acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04245108 |
| Source dataset | uspto-grants-1981_01 |
| ORD ID | ord-94cc084482774713b81d526f633a1324 |
| Source note | uspto-grants-1981_01 |