Isopropanol → HCID 575532, compound

HRID 1389720Notes

Reaction equation

HRID 1389720 reaction equation
C(O)(C)C.C[O-].[Na+].[CH:8]1[CH2:12][CH:11]=[CH:10][CH:9]=1.[C:13]1(=O)[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1>O>[CH2:13]1[CH2:18][CH2:17][C:16](=[C:9]2[CH:8]=[CH:12][CH:11]=[CH:10]2)[CH2:15][CH2:14]1

Participants

6

Reactant 4

HCID 3776IsopropanolHCID 7612CyclopentadieneHCID 7967CyclohexanoneHCID 10942334Sodium Methoxide

Product 1

HCID 575532HCID 575532, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

To a flask containing isopropyl alcohol (500 ml) and 25% sodiummethylate solution (10 g) are added a mixture of cyclopentadiene (150 g) and cyclohexanone (200 g) over a period of two hours. When addition is complete, the mixture is mixed with water and the organic layer extracted into hexane.

Workup

  1. additionare added
  2. additionWhen addition
  3. extractionthe organic layer extracted into hexane

Sources & evidence

ORD record
ord-9c606b56ec7f4e92bb5acb78e9f40237
Source dataset
uspto-grants-1981_01
Patent number
US04246167

Reaction notes

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